甲殼素合成實驗翻譯

2012-01-06 3:31 am
A 250 ml, three-necked round bottomed flask wascharged with 6.0 g ofCS and 60 ml of isopropyl alcohol, and the flask was fitted with a subsurfacenitrogen feed to remove dissolved oxygen from solutions. While stirring theslurry under nitrogen for 1 hour, a solution of 6.62 g VC in 25 ml of distilled water was prepared.This solution was then added to the CS slurry by syringe, and after 30 min, asolution of 26 ml of isopropyl alcohol and 11 ml of distilled water was added.After stirring for 2 additional h, the polymer was recovered under nitrogen.The polymer was washed under nitrogen once with a solution of 160 ml ofisopropyl alcohol and 40 ml of water, and once with 200 ml of isopropylalcohol. The light tan solid was brought to near dryness under a nitrogenstream. Finally, the product was dried at 40 0 under vacuum for 24h.

實驗怕做錯 麻煩大大幫忙翻譯一下,謝謝

回答 (2)

2012-01-06 2:41 pm
✔ 最佳答案
那些是甚麼鬼翻譯! 只是軟件直接翻的吧; 文中有些字似乎漏了空格&符號.

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1a. 往三頸圓底燒瓶注入60ml 的異丙醇和6.0g 的CS;
1b. 接駁喉管, 往液面之下通入氮氣 (以去除溶液中的溶氧).

2. 持續通入氮氣, 攪拌一小時.

3a. 製備VC 的溶液: 25ml 蒸餾水, 加入6.62g 的VC;
3b. 以針筒加入到[2]中的CS 的泥漿狀物.

4. 三十分鐘後, 加入異丙醇溶液: 26ml 異丙醇及11ml 蒸餾水 (不是分開加入, 而是先製成溶液, 再將溶液注入).

5. 再多拌兩小時(依然要通入氮氣), 製成聚合物.

6a. 仍然保持氮氣環境.
6b. 製備異丙醇溶液: 160ml 異丙醇 + 40ml 水; 以此溶液洗滌聚合物.
6c. 再用200ml 純異丙醇(不含水) 洗滌聚合物.

7a. 取得淺棕色固體.
7b. 在40度(??? 那是40還是400? 攝氏還是華氏或是開氏?) 以氮氣氣流吹乾成品, 維持廿四小時.


2012-01-06 06:44:41 補充:
呃, 原來three-necked flask 中文叫"三口瓶", 以前用英文讀書所以不知道.
2012-01-06 7:04 am
250毫升,三口圓底燒瓶6.0克離岸金融中心和60毫升的異丙醇,燒瓶 wascharged裝有一個 subsurfacenitrogen飼料刪除解決方案的溶解氧。雖然氮氣下攪拌1小時,解決了6.62克的VC在25毫升蒸餾水 theslurry prepared.This解決方案,然後用注射器加入到CS漿,後30分鐘,26毫升異丙醇 asolution11蒸餾水攪拌2額外 H added.After,高分子聚合物下nitrogen.The恢復氮氣下洗一次160毫升的ofisopropyl酒精和40毫升的水解決方案,並曾經與200毫升的異丙醇。駝色固體被帶到附近的乾燥下nitrogenstream。最後,該產品是在真空狀態下的400乾燥24小時。復原編輯


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